 Protein-Templated Quantum Dots
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Project Summary
Summary of Syntheses Attempted
| Date
|
Batch
|
Reaction Temp (C)
|
Reaction Time (hrs)
|
Notes
|
Gel Formation?
|
| 9/9/2014 |
JCS 1 |
23 |
11.58 |
no heating |
Not Attempted
|
| 9/16/2014 |
JCS 2 |
41 |
|
mantle setting 11 |
Not Attempted
|
| 9/23/2014 |
JCS 3 |
37 |
13.5 |
mantle setting 10 |
Not Attempted
|
| 9/30/2014 |
JCS 4 |
23 |
11.5 |
no heating |
Yes (first discovery)
|
| 9/30/2014 |
JCS 5 |
50 |
11.5 |
mantle setting 14.5 |
Yes
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| 10/7/2014 |
JCS 6 |
23 |
11 |
no heating |
Not Attempted
|
| 11/4/2014 |
JCS 7 |
23 |
|
no heating, BSA Control |
No (Structures did form but were noticeably different)
|
| 11/11/2014 |
JCS 8 |
23 |
7.5 |
Hg into BSA |
Not Attempted
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| 11/11/2014 |
JCS 9 |
23 |
7.5 |
BSA into Hg |
Not Attempted
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| 11/11/2014 |
JCS 10 |
Cold Room |
7.5 |
cold room synthesis- no change |
Not Attempted
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| 11/18/2014 |
JCS 11 |
23 |
48 |
attempting gel formation again |
Yes
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| 11/18/2014 |
JCS 12 |
23 |
48 |
attempting gel formation again |
Yes
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| 1/22/2015 |
JCS 13 |
23 |
|
No Mercury |
No
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| 1/29/2015 |
JCS 14 |
23 |
Over Weekend |
No Sodium Sulfide |
No (similar to BSA-only)
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| 2/4/2015 |
JCS 15 |
23 |
24 |
No BSA |
No (black precipitate)
|
| 2/5/2015 |
JCS 16 |
23 |
15 minutes |
original protocol with changed timeline |
Yes
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| 2/20/2015 |
JCS 17 |
23 |
15 minutes |
Decreased BSA conc (x10) |
No
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Protein-Templated Quantum Dots
