User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2014/12/05: Difference between revisions
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== | ==Objective== | ||
* | * Attempt gel formation using dried JCS 11 and JCS 12 syntheses | ||
==Protocol== | |||
# Add 2 mL of DI water to round bottom flask | |||
# Swirl Round bottom flask | |||
# After gel-film formation has been hydrated, add 10 additional mL of water | |||
# Swirl Round bottom flask | |||
# Structure should collapse into folded gels | |||
==Observations== | |||
Both JCS 11 and JCS 12 formed gels similar in appearance to JCS 4 and 5. However, not one of these look exactly like the other, which creates concern regarding the reproducibility of this synthesis batch-to-batch. | |||
Further analysis via pXRD and DSC is needed on all gels. | |||
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Revision as of 10:15, 9 December 2014
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Objective
Protocol
ObservationsBoth JCS 11 and JCS 12 formed gels similar in appearance to JCS 4 and 5. However, not one of these look exactly like the other, which creates concern regarding the reproducibility of this synthesis batch-to-batch. Further analysis via pXRD and DSC is needed on all gels. |