User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2014/12/05: Difference between revisions

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(Autocreate 2014/12/05 Entry for User:James_C._Schwabacher/Notebook/Protein-Templated_Quantum_Dots)
 
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==Entry title==
==Objective==
* Insert content here...
* Attempt gel formation using dried JCS 11 and JCS 12 syntheses


==Protocol==
# Add 2 mL of DI water to round bottom flask
# Swirl Round bottom flask
# After gel-film formation has been hydrated, add 10 additional mL of water
# Swirl Round bottom flask
# Structure should collapse into folded gels
==Observations==
Both JCS 11 and JCS 12 formed gels similar in appearance to JCS 4 and 5. However, not one of these look exactly like the other, which creates concern regarding the reproducibility of this synthesis batch-to-batch.
Further analysis via pXRD and DSC is needed on all gels.


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Revision as of 10:15, 9 December 2014

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Objective

  • Attempt gel formation using dried JCS 11 and JCS 12 syntheses

Protocol

  1. Add 2 mL of DI water to round bottom flask
  2. Swirl Round bottom flask
  3. After gel-film formation has been hydrated, add 10 additional mL of water
  4. Swirl Round bottom flask
  5. Structure should collapse into folded gels

Observations

Both JCS 11 and JCS 12 formed gels similar in appearance to JCS 4 and 5. However, not one of these look exactly like the other, which creates concern regarding the reproducibility of this synthesis batch-to-batch. Further analysis via pXRD and DSC is needed on all gels.