User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2014/09/23: Difference between revisions

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## pH was 9
## pH was 9
# Time reaction started: 12pm
# Time reaction started: 12pm
# Mantle Setting: 10. Temperature: 37 °C


==Precipitation Protocol==
==Precipitation Protocol==

Revision as of 18:10, 24 September 2014

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Objective

  • Start new QD synthesis at a lower temperature
  • Acquire UVVIS and fluorescence emission data
  • Continue precipitation of JCS 1 and JCS 2

Synthesis Protocol

  1. Create 15 mg/mL solution of BSA in HPLC grade water
    1. .1540 g of BSA in 10.267 mL of water
  2. Add 5 mL of BSA solution and 5 mL of previously prepared 5mM HgNO3 solution
  3. Add 60 μL of ~1M NaOH to reaction while stirring
    1. pH was 9
  4. Time reaction started: 12pm
  5. Mantle Setting: 10. Temperature: 37 °C

Precipitation Protocol


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