User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2014/09/17: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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== | ==Objective== | ||
* | * Complete the QD synthesis begun yesterday | ||
* Begin precipitation of JCS 1 and JCS 2 | |||
==Protocol== | |||
# Create 20 mM sodium sulfide solution | |||
## .024018 g of Sodium Sulfide (MW=240.18) needed for 5 mL | |||
## Used .1415 g of Sodium Sulfide used (in 10 mL) because the sample is contaminated with excess water | |||
# Add 4 mL of 20 mM sodium sulfide solution to reaction | |||
## Allowed the mixture to stir vigorously for 15 minutes | |||
## Poured contents (minus the stir bar) into a darkened falcon tube, to be stored at room temperature | |||
## total synthesis time: 12 hrs + 15 minutes for Sodium Sulfide addition | |||
# Removed 1 mL aliquot from JCS 2 for future testing with UVVIS and Fluorescence | |||
# Added ~40 mL of 200 proof ethanol to each falcon tube (JCS 1 and JCS 2) | |||
# Placed the samples in the freezer. I will check on Friday to see if any precipitation has occurred. | |||
Latest revision as of 00:19, 27 September 2017
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