User:James C. Schwabacher/Notebook/CHEM-571/2014/02/05: Difference between revisions
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# The solution is stirred for 20 minutes | # The solution is stirred for 20 minutes | ||
# The solution is then aged at 50C under air for 2 hours. | # The solution is then aged at 50C under air for 2 hours. | ||
==Results== | |||
[[Image:BSA-CYS.png|750px]] | |||
[[Image:02.12.UV-Vis.BSA-GSH.png|750px]] | |||
==Notes== | ==Notes== | ||
* 2.53 mL of 1M NaOH, in the future 2mL will be added to adjust the pH. | * 2.53 mL of 1M NaOH, in the future 2mL will be added to adjust the pH. | ||
*When first adding NaOH it resulted in a cloudy white precipitate, that increased in cloudiness as more NaOH was added, after the last mL was added the solution changed to a clear gold solution. | *When first adding NaOH it resulted in a cloudy white precipitate, that increased in cloudiness as more NaOH was added, after the last mL was added the solution changed to a clear gold solution. | ||
Revision as of 11:40, 5 March 2014
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Protocol
Preparation of 10uM GSH
Protocol for New synthesis methodThis protocol was taken from Matt Harting's notebook
ResultsNotes
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