User:Ellen Petersen/Notebook/MOF Continued/2013/04/09

From OpenWetWare

(Difference between revisions)
Jump to: navigation, search
Line 17: Line 17:
* 6.) Run Powder X- Diffraction  
* 6.) Run Powder X- Diffraction  
 +
 +
[[Image:041113.png‎|200px|PPF-18]]

Revision as of 10:41, 3 July 2013

MOF :Tara Main project page
Previous entry      Next entry

PPF-18

  • 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089 g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial
  • 2.) Add 1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL)
  • 3.) Sealed and Sonicated to ensure homogeneity
  • 4.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)

_____________________________________________________________________________________________________________________________________________ 04-11-2013

  • 5.) Vacuum Filtration
  • 6.) Run Powder X- Diffraction


PPF-18



Personal tools