User:Ellen Petersen/Notebook/MOF Continued/2013/04/02: Difference between revisions

From OpenWetWare
Jump to navigationJump to search
(Autocreate 2013/04/02 Entry for User:Ellen_Petersen/Notebook/MOF_Continued)
 
No edit summary
Line 6: Line 6:
| colspan="2"|
| colspan="2"|
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
==Entry title==
==DPNI==
* Insert content here...
 
* 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.4025 g, 3.00 mmol) and 4-aminopyridine (.4235 g, 6.00 mmol)to round bottom flask
* 2.) Add 75 mL of solvent (DMA) ~keep under hood~
* 3.) Add Stir Bar to solution
* 4.) Put under spout and raise black knob until there is enough pressure to hold it in place
* 5.) Begin to stir
* 6.) If attached to condenser, turn on water very slightly
* 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up)
* 8.) Turn on heat to 40, switch down accordingly until it reaches 135 degrees consistently.
______________________________________________________________________________________________________
 
04-03-13
 
* 9.) Turn off nitrogen and water, Cool to Room Temperature
* 10.) Filter out solid using diethyl ether
* 11.) NMR in Chloroform (See Image Below)
 




Revision as of 08:46, 28 June 2013

Project name <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

DPNI

  • 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.4025 g, 3.00 mmol) and 4-aminopyridine (.4235 g, 6.00 mmol)to round bottom flask
  • 2.) Add 75 mL of solvent (DMA) ~keep under hood~
  • 3.) Add Stir Bar to solution
  • 4.) Put under spout and raise black knob until there is enough pressure to hold it in place
  • 5.) Begin to stir
  • 6.) If attached to condenser, turn on water very slightly
  • 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up)
  • 8.) Turn on heat to 40, switch down accordingly until it reaches 135 degrees consistently.

______________________________________________________________________________________________________

04-03-13

  • 9.) Turn off nitrogen and water, Cool to Room Temperature
  • 10.) Filter out solid using diethyl ether
  • 11.) NMR in Chloroform (See Image Below)



Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Ellen_Petersen/Notebook/MOF_Continued/2013/04/02&oldid=705829"