User:Ellen Petersen/Notebook/MOF Continued/2013/04/02: Difference between revisions
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* 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.4025 g, 3.00 mmol) and 4-aminopyridine (.4235 g, 6.00 mmol)to round bottom flask | |||
* 2.) Add 75 mL of solvent (DMA) ~keep under hood~ | |||
* 3.) Add Stir Bar to solution | |||
* 4.) Put under spout and raise black knob until there is enough pressure to hold it in place | |||
* 5.) Begin to stir | |||
* 6.) If attached to condenser, turn on water very slightly | |||
* 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up) | |||
* 8.) Turn on heat to 40, switch down accordingly until it reaches 135 degrees consistently. | |||
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* 9.) Turn off nitrogen and water, Cool to Room Temperature | |||
* 10.) Filter out solid using diethyl ether | |||
* 11.) NMR in Chloroform (See Image Below) | |||
Revision as of 08:46, 28 June 2013
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DPNI
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