User:Ellen Petersen/Notebook/MOF Continued/2013/03/06

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Remove amorphous material in PPF-18 & Synthesizing Sheets

  • 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
  • 2.) Add .0092 g to small vial
  • 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
  • Powder X-Ray Diffraction taken of PPF-18, and PPF-18 with adenine


PPF-18

PPF-18 with Adenine

PPF-18 with Adenine _________________________________________________________________________________________________________________ 03-06-13

  • Synthesizing Sheets:
  • 1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
  • 2.) Sonification
  • 3.) Heat 24 hours, cool down 9 hours

03-19-13

  • 4.) Filtration

03-20-13

  • 5.) Powder X-Ray Diffraction (See Image 1 below)

Sheets



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