User:Ellen Petersen/Notebook/MOF Continued/2013/03/06

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(Remove amorphous material in PPF-18)
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03-06-13
03-06-13
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* 4.)
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*Synthesizing Sheets:
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*1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
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*2.) Sonification
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*3.) Heat 24 hours, cool down 9 hours
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03-19-13
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*4.) Filtration
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03-20-13
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*5.) Powder X-Ray Diffraction (See Image 1 below)
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[[Image:032013.png‎|200px|Description of image]]
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03-08-13
03-08-13

Revision as of 09:16, 28 June 2013

MOF: Tara Main project page
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Remove amorphous material in PPF-18

  • 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
  • 2.) Add .0092 g to small vial
  • 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine

_________________________________________________________________________________________________________________ 03-06-13

  • Synthesizing Sheets:
  • 1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
  • 2.) Sonification
  • 3.) Heat 24 hours, cool down 9 hours

03-19-13

  • 4.) Filtration

03-20-13

  • 5.) Powder X-Ray Diffraction (See Image 1 below)

Image:032013.png

03-08-13

  • 4.)Filter


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