User:Ellen Petersen/Notebook/MOF/2013/07/17

From OpenWetWare

< User:Ellen Petersen | Notebook | MOF | 2013 | 07(Difference between revisions)
Jump to: navigation, search
(Autocreate 2013/07/17 Entry for User:Ellen_Petersen/Notebook/MOF)
Current revision (15:20, 8 August 2013) (view source)
 
Line 6: Line 6:
| colspan="2"|
| colspan="2"|
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
-
==Entry title==
+
==PPF-18 w/ Zinc Nitrate==
-
* Insert content here...
+
*1.) Add Zinc nitrate hexahydrate (.00593 g, .03 mmol), N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol),1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL), & 100μl Zinc Nitrate Porphyrin Mix to a small capped vial labeled PPF-18 w/ Cupric Acetate
 +
*2.) Sealed and sonicated to ensure homogeneity
 +
*3.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)
 +
 
 +
_____________________________________________________________________________________________________________________________________________
 +
07-18-2013
 +
 +
* 9.) Vacuum Filtration
 +
*10.) Powder X-Ray Diffraction (see images below)
 +
 

Current revision

Project name Main project page
Previous entry      Next entry

PPF-18 w/ Zinc Nitrate

  • 1.) Add Zinc nitrate hexahydrate (.00593 g, .03 mmol), N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol),1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL), & 100μl Zinc Nitrate Porphyrin Mix to a small capped vial labeled PPF-18 w/ Cupric Acetate
  • 2.) Sealed and sonicated to ensure homogeneity
  • 3.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)

_____________________________________________________________________________________________________________________________________________ 07-18-2013

  • 9.) Vacuum Filtration
  • 10.) Powder X-Ray Diffraction (see images below)



Personal tools