User:Ellen Petersen/Notebook/MOF/2013/07/08: Difference between revisions

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==Entry title==
==PPF-18 & PPF-20==
* Insert content here...
* 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine  (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089  g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial
* 2.) Add 1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL)
* 3.) Sealed and Sonicated to ensure homogeneity
* 4.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)
* 5.) Add solids to a second vial 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine  (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089  g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0168 g, .01 mmol)to small capped vial
* 6.) Add 1.0 M nitric acid (30 μL, .05 mmol) in ethanol, N,N-dimethyl formamide (DMF)(1.5 mL),Ethanol (0.5 mL)
* 7.) Sealed and Sonicated to ensure homogeneity
* 8.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)




Revision as of 13:04, 8 July 2013

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PPF-18 & PPF-20

  • 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089 g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial
  • 2.) Add 1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL)
  • 3.) Sealed and Sonicated to ensure homogeneity
  • 4.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)
  • 5.) Add solids to a second vial 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089 g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0168 g, .01 mmol)to small capped vial
  • 6.) Add 1.0 M nitric acid (30 μL, .05 mmol) in ethanol, N,N-dimethyl formamide (DMF)(1.5 mL),Ethanol (0.5 mL)
  • 7.) Sealed and Sonicated to ensure homogeneity
  • 8.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2)



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