User:Ellen Petersen/Notebook/MOF/2013/06/28: Difference between revisions

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*1.) Due to a shortage of Diethyl ether I attempted to use THF to wash a small amount of the DPNI
*1.) Due to a shortage of Diethyl ether I attempted to use THF to wash a small amount of the DPNI
*2.) Add 20 mL of DPNI to 50 mL of THF
*2.) Add 20 mL of DPNI to 50 mL of THF
*3.) vacuum filtration
*3.) Vacuum filtration
*4.) Result: Not the same as Diethyl ether, much more watered down and much less solid.  
*4.) Result: Not the same as Diethyl ether, much more watered down and much less solid.  



Revision as of 10:53, 28 June 2013

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DPNI

  • 1.) Due to a shortage of Diethyl ether I attempted to use THF to wash a small amount of the DPNI
  • 2.) Add 20 mL of DPNI to 50 mL of THF
  • 3.) Vacuum filtration
  • 4.) Result: Not the same as Diethyl ether, much more watered down and much less solid.