User:Ellen Petersen/Notebook/MOF/2013/06/26: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF</span> | ||
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== | ==DPNI: 06-26-13== | ||
* | |||
* 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805 g, 3.00 mmol) and 4-aminopyridine (.847 g, 6.00 mmol)to round bottom flask (I added .8054 g of 1,4,5,8 Naphthalenetetracarboxylic dianhydride, and .8479 g of 4-aminopyridine) | |||
* 2.) Add 150 mL of solvent (DMA) ~keep under hood~ | |||
* 3.) Add Stir Bar to solution | |||
* 4.) Put under spout and raise black knob until there is enough pressure to hold it in place | |||
* 5.) Begin to stir | |||
* 6.) If attached to condenser, turn on water very slightly | |||
* 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up) | |||
* 8.) Turn on heat to 50, switch down accordingly until it reaches 135 degrees consistently. | |||
* 9.) If solution seems to be boiling adjust and turn down | |||
* 10.) Solution stable at 135 degrees at 35, mark red line on it to see difference in solution level. | |||
______________________________________________________________________________________________________ | |||
06-27-13 | |||
* 11.) Turn off nitrogen and water, Cool to Room Temperature | |||
* 12.) Not enough diethyl ether, took 400 mL of diethyl ether (instead of the required 600 mL) and poured 2/3's of DPNI solution into the 400 mL of diethyl ether. | |||
* 13.) Filter out | |||
______________________________________________________________________________________________________ | |||
07-02-13 | |||
*14.) Ran 1/4 of the DPNI with 150 mL of ethanol through the rotavap | |||
______________________________________________________________________________________________________ | |||
07-05-13 | |||
*15.) Ran the rest of the DPNI with 150 mL of ethanol through the rotavap | |||
Revision as of 12:59, 8 July 2013
MOF | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
DPNI: 06-26-13
______________________________________________________________________________________________________ 06-27-13
______________________________________________________________________________________________________ 07-02-13
______________________________________________________________________________________________________ 07-05-13
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