User:Ellen Petersen/Notebook/MOF/2012/04/16

< User:Ellen Petersen | Notebook | MOF | 2012 | 04(Difference between revisions)

Current revision

Project name

1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805 g, 3.00 mmol) and 4-aminopyridine (.847 g, 6.00 mmol)to round bottom flask
2.) Add 150 mL of solvent (DMA) ~keep under hood~
3.) Add Stir Bar to solution
4.) Put under spout and raise black knob until there is enough pressure to hold it in place
5.) Begin to stir
6.) Vacuum out oxygen : turn big end of nossle up, observe that solution does react
7.) Turn off vacuum and turn on nitrogen: turn little end of nossle up. Bubbles in back should appear, this means nitrogen is on
8.) Turn on heat to 56, switch down accordingly until it reaches 135 degrees consistently.
9.) If solution seems to be boiling adjust and turn down
10.) Solution stable at 133 degrees at 51, mark red line on it to see difference in solution level.

@@ Line 6: / Line 6: @@
 | colspan="2"|
 <!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
-==Entry title==
+==April 16, 2012==
-* Insert content here...
+* 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805 g, 3.00 mmol) and 4-aminopyridine (.847 g, 6.00 mmol)to round bottom flask
+* 2.) Add 150 mL of solvent (DMA) ~keep under hood~
+* 3.) Add Stir Bar to solution
+* 4.) Put under spout and raise black knob until there is enough pressure to hold it in place
+* 5.) Begin to stir
+* 6.) Vacuum out oxygen : turn big end of nossle up, observe that solution does react
+* 7.) Turn off vacuum and turn on nitrogen: turn little end of nossle up. Bubbles in back should appear, this means nitrogen is on
+* 8.) Turn on heat to 56, switch down accordingly until it reaches 135 degrees consistently.
+* 9.) If solution seems to be boiling adjust and turn down
+*10.) Solution stable at 133 degrees at 51, mark red line on it to see difference in solution level.