User:Ellen Petersen/Notebook/MOF/2012/04/12
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| - | == | + | ==DPNI Take 1== |
| - | * | + | * 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) |
| + | *2.) 4- aminopyridine (.847 g, 6.00 mmol) | ||
| + | *3.) Diethyl ether (600 mL | ||
| + | *4.) Dimethylacetamide (DMA) (150 mL) | ||
| + | |||
| + | Dissolve 1&2 in DMA stirred at 135 degrees C overnight | ||
| + | cooled to room temperature and poured onto diethyl ether (600 mL) | ||
| + | |||
| + | precipitate filter and washed with diethyl ether | ||
| + | dried under vacuum to yield | ||
| + | |||
Revision as of 23:57, 4 February 2013
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DPNI Take 1
Dissolve 1&2 in DMA stirred at 135 degrees C overnight cooled to room temperature and poured onto diethyl ether (600 mL) precipitate filter and washed with diethyl ether dried under vacuum to yield
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