User:Ellen Petersen/Notebook/MOF/2012/04/12: Difference between revisions

From OpenWetWare
< User:Ellen Petersen‎ | Notebook‎ | MOF‎ | 2012‎ | 04
Jump to navigationJump to search
No edit summary
Line 6: Line 6:
| colspan="2"|
| colspan="2"|
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
==DPNI Take 1==
==DPNI: 04-12-12==
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
*2.) 4- aminopyridine (.847 g, 6.00 mmol)
*2.) 4- aminopyridine (.847 g, 6.00 mmol)

Revision as of 05:40, 25 June 2013

Project name <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

DPNI: 04-12-12

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)
  • Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
  • Cooled to room temperature and poured onto diethyl ether (600 mL).
  • Precipitate filter and washed with diethyl ether
  • dried under vacuum to yield



Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Ellen_Petersen/Notebook/MOF/2012/04/12&oldid=704959"