User:Eleni N. Kalivas/Notebook/CHEM-571/2014/11/05: Difference between revisions

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(Autocreate 2014/11/05 Entry for User:Eleni_N._Kalivas/Notebook/CHEM-571)
 
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==Entry title==
==Objective==
* Insert content here...
*weigh out PVAC ribbons and soak in 20 ppm Malachite Green and UV-vis in 10 min increments
*Prepare dried PVAC ribbons for pXRD and DSC
*Begin new bead synthesis for PVAC


==Protocol==
#The Malachite Green solution was made and after UV-vis was found to be at a concentration of 20.2ppm
##Dilution of .5mL of 20ppm into 5mL for a total concentration of 2ppm total to be measured with UV-vis
##1.4163g of PVAC ribbons were placed into 10 mL of 20ppm Malachite Green Solution
#DSC preparation
##Tzero Pan weight: 0.04192g
##Tzero Pan and PVAC ribbons weight: 0.04494g
##Tzero Pan, PVAC ribbons and Lid weight: 0.05539g
#pXRD Preparation: Take dried PVAC ribbons and condense them onto a pXRD plate
#New Bead Synthesis
##
==Data==
*UV-Vis of PVAC Ribbon absorptions of Malachite Green


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Revision as of 08:29, 5 November 2014

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Objective

  • weigh out PVAC ribbons and soak in 20 ppm Malachite Green and UV-vis in 10 min increments
  • Prepare dried PVAC ribbons for pXRD and DSC
  • Begin new bead synthesis for PVAC

Protocol

  1. The Malachite Green solution was made and after UV-vis was found to be at a concentration of 20.2ppm
    1. Dilution of .5mL of 20ppm into 5mL for a total concentration of 2ppm total to be measured with UV-vis
    2. 1.4163g of PVAC ribbons were placed into 10 mL of 20ppm Malachite Green Solution
  2. DSC preparation
    1. Tzero Pan weight: 0.04192g
    2. Tzero Pan and PVAC ribbons weight: 0.04494g
    3. Tzero Pan, PVAC ribbons and Lid weight: 0.05539g
  3. pXRD Preparation: Take dried PVAC ribbons and condense them onto a pXRD plate
  4. New Bead Synthesis

Data

  • UV-Vis of PVAC Ribbon absorptions of Malachite Green