User:Eleni N. Kalivas/Notebook/CHEM-571/2014/09/19: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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==Objective== | |||
# Start Analysis on pXRD spectra | |||
# new PVA and 10% PVA-clay synthesis | |||
# set up new experiments with PVA and PVA-clay films soaking in Arsenic (As) and Mercury (Hg) each with 150ppm, 100ppm, 50ppm | |||
==Protocol== | ==Protocol== | ||
====Synthesis of new films==== | ====Synthesis of new films==== | ||
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| As stock solution (ppm) ||3738.61 | | As stock solution (ppm) ||3738.61 | ||
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| As 150ppm solution || | | As 150ppm solution ||4mL stock in 100mL | ||
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| As 100ppm Solution || | | As 100ppm Solution ||2.76mL stock in 100mL | ||
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| As 50ppm solution|| | | As 50ppm solution||1.32mL stock in 100mL | ||
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| Hg stock solution (ppm) ||268 | | Hg stock solution (ppm) ||268 | ||
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# The vial was placed into a oven in order to remove any excess hydrate | # The vial was placed into a oven in order to remove any excess hydrate | ||
==Data== | |||
====XRD analysis of PVA film soaked in 80ppm Malachite Green==== | |||
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Latest revision as of 00:19, 27 September 2017
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Objective
ProtocolSynthesis of new filmsSynthesis is the same that was used on August 26th, 2014
1.0037g PVA and 0.1099g NaMT clay
0.9998g PVA PVA and PVA-clay in Hg and AsMass of films in each vial
PVA-Clay Cation Exchange
DataXRD analysis of PVA film soaked in 80ppm Malachite Green |