User:Eleni N. Kalivas/Notebook/CHEM-571/2014/09/12: Difference between revisions
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==Protocol== | ==Protocol== | ||
*Exfoliated Clays | |||
Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014. | Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014. | ||
*Powder Xray diffraction | |||
Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison. | Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison. | ||
*Preparation of new Malachite Green (M.G.) solutions. | |||
##200 ppm M.G. made by [[User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12|Madeline Bee]] and calculations can be found on her page. | ##200 ppm M.G. made by [[User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12|Madeline Bee]] and calculations can be found on her page. | ||
##80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask. | ##80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask. |
Revision as of 11:39, 12 September 2014
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Objective
Protocol
Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014.
Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison.
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