User:Eleni N. Kalivas/Notebook/CHEM-571/2014/09/03: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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*DSC Spectra
*DSC Spectra


*FTIR spectra
====FTIR spectra====
Polymer Film
[[Image:PVA_film_FTIR_graph.PNG|750px]]


Polymer-Clay Film
[[Image:PVAC_film_FTIR_graphs.PNG|750px]]


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Latest revision as of 00:13, 27 September 2017

Project name Main project page
Previous entry      Next entry

Objective

  • Finish the film synthesis from Friday, August 29
  • Start a new film synthesis
  • DSC analysis of soaked films
  • FTIR analysis of soaked films

Protocol

  • Finish the film synthesis
  1. follow the protocol from Friday August 29th
  • Start new synthesis of Polymer and Polymer-clay films
  1. Using the synthesis method from Tuesday, August 26
  • DSC
  1. weigh pan and cap separately, record weight
  2. weigh out approximately 0.3mg of each film
  3. place then into a pan, and seal cap over each
    1. 10 samples total
      1. 4 polymer films that have been soaked in 2ppm, 8ppm, 80ppm, and 200ppm
      2. 4 polymer-clay films that have been soaked in 2ppm, 8ppm, 80ppm, and 200ppm
      3. 1 plane polymer film soaking in water, and 1 plane polymer-clay films soaking in water
  4. Input data information into the computer program (weights, position, reference)
  5. Place prepared capped trays into the machine and run analysis


  • Tables of DSC preparation
Mass of Pan + Lid Mass of PVA + Clay + MG Concentration
0.05311 0.00312 2ppm
0.05234 0.00324 8ppm
0.05248 0.0042 80ppm
0.05213 0.00499 200ppm
Mass of Pan + Lid Mass of PVA + MG Concentration
0.05287 0.00385 2ppm
0.05269 0.00499 8ppm
0.05294 0.00316 80ppm
0.05285 0.00365 200pm
Mass of Pan + Lid Mass of PVA
0.0527 0.00572
Mass of Pan + Lid Mass of PVA + Clay
0.05248 0.0069

Data

  • DSC Spectra

FTIR spectra

Polymer Film

Polymer-Clay Film


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