User:Dhea Patel/Notebook/Hemoglobin Project/2013/06/11

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<b>Mb/Tris in Acetonitrile</b>
<b>Mb/Tris in Acetonitrile</b>
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[[Image:Mb_Tris1_OPD_H2O2_MeCN_FILTERED_WORKUP_GRAPH.png]]
+
[[Image:Mb_Tris1_OPD_H2O2_MeCN_FILTERED_WORKUP_GRAPH.png|750px]]
Note: The source was off during the 80mins measurement, so data was not available.  
Note: The source was off during the 80mins measurement, so data was not available.  
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[[Image:Mb_Tris2_OPD_H2O2_MeCN_WORKUP_GRAPH.png]]
+
[[Image:Mb_Tris2_OPD_H2O2_MeCN_WORKUP_GRAPH.png|750px]]
<b>Mb/Phosphate in Acetone</b>
<b>Mb/Phosphate in Acetone</b>
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[[Image:Mb_Phosphate_OPD_H2O2_Acetone_WORKUP_GRAPH.png]]
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[[Image:Mb_Phosphate_OPD_H2O2_Acetone_WORKUP_GRAPH.png|750px]]
<b>Mb/Acetate in Acetone</b>
<b>Mb/Acetate in Acetone</b>
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[[Image:Mb_Acetate_OPD_H2O2_Acetone_WORKUP_GRAPH.png]]
+
[[Image:Mb_Acetate_OPD_H2O2_Acetone_WORKUP_GRAPH.png|750px]]
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Reaction of OPD+H2O2 with Mb Catalyst in Acetonitrile Suspension

The procedurefor the reaction of OPD and H2O2 was followed using a Mb/Tris catalyst and an acetonitrile suspension. Like yesterday, the reaction was run in a beaker with a stir bar and the solution was filtered before taking a spectrum.

In addition reactions were run using Mb/Phosphate and Mb/Acetate in acetone suspension. Because the acetone corroded the plastic, samples 80mins-140mins are taken without filtering the sample.

Data

Mb/Tris in Acetonitrile

Note: The source was off during the 80mins measurement, so data was not available.


Mb/Phosphate in Acetone

Mb/Acetate in Acetone


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