User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/05
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Purification of Large-Scale Reaction Between CNP & MTTThe procedure for the reaction being discussed can be found here. Procedure:
EtOAc Fraction: File:Awl etoac fraction 100515.pdf MeOH Fraction: File:Awl meoh fraction 100515.pdf The EtOAc fraction shows a clear peak at 287, which is a predicted mass for the desired product (the molar weight + a sodium ion). A likely next step is to run a TLC on the compound in an attempt at further purification. |