User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/02: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
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##After the fraction collected with ethyl acetate was obtained, another flask was used to collect a methanol fraction. | ##After the fraction collected with ethyl acetate was obtained, another flask was used to collect a methanol fraction. | ||
#Mass spectrometry was used to examine the two fractions. The result is shown below: | #Mass spectrometry was used to examine the two fractions. The result is shown below: | ||
XXX | |||
'''Procedure for large-scale rxn:''' | '''Procedure for large-scale rxn:''' |
Latest revision as of 01:13, 27 September 2017
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Purification of Product of Rxn Between MTT and CNP, and Large-Scale Reaction SetupNote that MTT refers to 5-(methylthio)-1,3,4-thiadiazole-2-thiol, and that CNP refers to 2-chloro-3-nitropyridine. Structures shown here Goals:
Procedure for purification:
XXX Procedure for large-scale rxn:
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