User:Andrew K Farag/Notebook/CHEM-581/2014/09/17: Difference between revisions
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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span> | |style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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*Measure MG new data through UV-Vis | *Measure MG new data through UV-Vis | ||
*Film Processing | *Film Processing | ||
*Filter stirring clay | *Filter stirring clay in centriuge | ||
*Set up PXRD | **4000rpm for 30 minutes at 4C for original separation | ||
**with water then ethanol for 10 minutes | |||
**repeat for another cycle and dried done by Dr. Hartings | |||
*Set up PXRD of PVA+Clay films at different concentrations | |||
#1-Clay powder-control | |||
#2-8ppm by Madeleleine | |||
#3-2ppm by | |||
#4-PVA film-control | |||
#5-80ppm by Eleni | |||
#6-200ppm by my group | |||
## Instrument Settings | |||
### 2<sup>o</sup> start angle | |||
### 40<sup>o</sup> stop angle | |||
### 1<sup>o</sup>/second scan speed (this seems too fast, will check on this) | |||
### 0.5<sup>o</sup> sampling width | |||
==Calculations== | ==Calculations== | ||
*Dilutions of MG solutions | *Dilutions of MG solutions | ||
**200ppm*0.2mL=8ppm*5mL | **200ppm*0.2mL=8ppm*5mL(vial with PVA film) | ||
**80ppm*0.5mL=8ppm*5mL | **80ppm*0.5mL=8ppm*5mL(vial with no film) | ||
**80ppm*0.2mL=8ppm*2mL(vial with PVA film) | |||
==Figures== | |||
Figure 1. Shows the separation of the clay after the first washing of water. | |||
[[Image:washing1.png]] | |||
Figure 2. Shows the dried clay being collected for future testing. | |||
[[Image:dry.png]] | |||
==Results== | |||
[[Image:Uvavis.png]] | |||
[[Image:ICE table PVA+control.png]] |
Latest revision as of 00:18, 27 September 2017
Biomaterials Design Lab | Main project page Previous entry Next entry |
Description
Calculations
FiguresFigure 1. Shows the separation of the clay after the first washing of water. Figure 2. Shows the dried clay being collected for future testing. Results |