User:Alicia Rasines Mazo/Notebook/CHEM-581 Experimental Chemistry I/2014/10/29: Difference between revisions

From OpenWetWare
Jump to navigationJump to search
No edit summary
No edit summary
Line 20: Line 20:
* 0.1050 g of Na<sup>+</sup>MT and 0.9930 g 22,000 PVA in 4 mL of 0.12 M HCl.
* 0.1050 g of Na<sup>+</sup>MT and 0.9930 g 22,000 PVA in 4 mL of 0.12 M HCl.
* Stirred gently at 90ºC until all crystals dissolved.
* Stirred gently at 90ºC until all crystals dissolved.
* Poured dissolved crystals into mixture of glutaraldehyde and hexane solvent.
* Poured dissolved crystals solution into hexane. They formed drops at first but dissolved with time. Our sample was to concentrated to be of use
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
|}
|}


__NOTOC__
__NOTOC__

Revision as of 08:09, 29 October 2014

Project name <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

Tasks for October 29

  • Bead synthesis

Bead synthesis

  • 7 mL of 10% HCl (1.2 M) were added to 1.0015 g of 22,000 PVA and 0.1099 g of Na+MT 7 mL of 0.2 M Na2SO4
  • Stirred gently at room temperature until all crystals were dissolved.
  • Added 0.5 mL of 0.8% glutaraldehyde.
  • Stirred for a futher 3 min to ensure homogeneity

Note: this technique cannot be used because the components solidify before you can pour the drops into acetone to make beads.

Second technique:

  • 0.1050 g of Na+MT and 0.9930 g 22,000 PVA in 4 mL of 0.12 M HCl.
  • Stirred gently at 90ºC until all crystals dissolved.
  • Poured dissolved crystals solution into hexane. They formed drops at first but dissolved with time. Our sample was to concentrated to be of use


Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Alicia_Rasines_Mazo/Notebook/CHEM-581_Experimental_Chemistry_I/2014/10/29&oldid=839706"