User:Alicia Rasines Mazo/Notebook/CHEM-581 Experimental Chemistry I/2014/09/17: Difference between revisions
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===Completing preparation of ionic liquid modified clay=== | ===Completing preparation of ionic liquid modified clay=== | ||
Continued from [http://openwetware.org/wiki/User:Alicia_Rasines_Mazo/Notebook/CHEM-581_Experimental_Chemistry_I/2014/09/10 Sept.10] | Continued from [http://openwetware.org/wiki/User:Alicia_Rasines_Mazo/Notebook/CHEM-581_Experimental_Chemistry_I/2014/09/10 Sept.10] | ||
# | # Centrifuge: 4000 rpm, 30 min, 4°C | ||
# | #*Solution starting weight: 27.45 g | ||
#*Collect supernatant first time | |||
#*Wash with H<sub>2</sub>O | |||
#*Wash with EtOH | |||
#*Wash with H<sub>2</sub>O | |||
#*Wash with EtOH | |||
# Dry in oven at 90C overnight | # Dry in oven at 90C overnight | ||
# Grind with a mortar and pestle | # Grind with a mortar and pestle | ||
# Store in a dessicator | # Store in a dessicator | ||
====pXRD Measurements==== | |||
*Sample prepped on [http://openwetware.org/wiki/User:Alicia_Rasines_Mazo/Notebook/CHEM-581_Experimental_Chemistry_I/2014/09/12 Sept. 12], to be analysed on Sept. 19. | |||
*# Hartings- NaMT | |||
*# Madeleine and Alicia- 8 ppm | |||
*# James's group- 2 ppm | |||
*# James's group- PVA | |||
*# Eleni's group- 80 ppm | |||
*# Andrew's group- 200 ppm | |||
*Instrument parameters on Dr Hartings OWW | |||
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Revision as of 08:58, 17 September 2014
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Tasks for 17 September
UV-Vis analysis of MG leftover solutions
Completing synthesis of 10% PVA-exfoliated clayContinued from Sept. 12
Completing preparation of ionic liquid modified clayContinued from Sept.10
pXRD Measurements
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