User:Abigail E. Miller/Notebook/MOF Project/2013/01/31

Current revision

Metal Organic Frameworks

made a solution of 4, 4 bipyridine
- 6 mg of 4, 4' bipyridine in 3 mL of DEF and 1 mL of ethanol

exchange the pillar from DPNI to 4, 4' bipyridine
- 1:15 pm mixed 3 mL of hte above solution with 13 mg of PPF-18
- 4:30 pm filtered and dried the crystals

see Eleni's notebook for 3 vials of reactants for synthesizing PPF-18
- place the vials in the oven at 9am on 2/1/2013 to ehat for 24 hrs at 85 °C then cool to room temp over for 9 hrs.

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 ==Bench Work==
-* Insert content here...
+* made a solution of 4, 4 bipyridine
+** 6 mg of 4, 4' bipyridine in 3 mL of DEF and 1 mL of ethanol
+* exchange the pillar from DPNI to 4, 4' bipyridine
+** 1:15 pm mixed 3 mL of hte above solution with 13 mg of PPF-18
+** 4:30 pm filtered and dried the crystals
+*see Eleni's notebook for 3 vials of reactants for synthesizing PPF-18
+** place the vials in the oven at 9am on 2/1/2013 to ehat for 24 hrs at 85 °C then cool to room temp over for 9 hrs.
+* react OD2A with zinc nitrate
+** see Matt's notebook for reactant amounts
+** heated for 2 hrs at 130 °C
+** let cool on bench top - some white crystals at hte bottom of hte vial
+**heated from 1-4:30pm at 130 °C
+** then turned off the oven and let it cool to room temp
+*
 ==Data/Spectra==