User:Abigail E. Miller/Notebook/MOF Project/2013/01/25

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(Objective)
Current revision (11:50, 29 January 2013) (view source)
 
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==Bench Work==
==Bench Work==
-
* Insert content here...
+
====exchanging PPF-18 with guanine and adenine====
 +
*
 +
 
 +
====synthesizing PPF-18 and PPF-20====
 +
* Added zinc nitrate hexahydrate, DPNI and TCPP to four vials.
 +
** insert chart with weights here
 +
 
 +
*added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4
 +
** made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4
 +
** added 250 μL of pure ethanol to vials 1-3
 +
 
 +
*made a 10 mL solution of 1 M nitric acid in ethanol
 +
** 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid
 +
** --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol
 +
 
 +
* added 100 μL of 1M HNO3 in EtOH to vials 1&2 and 80 μL to vials 3&4
 +
 
 +
* sonciated vials and placed in oven at 3pm
 +
** programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs
==Data/Spectra==
==Data/Spectra==

Current revision

Metal Organic Frameworks Main project page
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Objective

  • Synthesis of PPF18 and PPF20
  • exchange PPf18 with adenine and guanine
  • make a stock solution of 1M HNO3 in ethanol

Bench Work

exchanging PPF-18 with guanine and adenine

synthesizing PPF-18 and PPF-20

  • Added zinc nitrate hexahydrate, DPNI and TCPP to four vials.
    • insert chart with weights here
  • added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4
    • made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4
    • added 250 μL of pure ethanol to vials 1-3
  • made a 10 mL solution of 1 M nitric acid in ethanol
    • 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid
    • --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol
  • added 100 μL of 1M HNO3 in EtOH to vials 1&2 and 80 μL to vials 3&4
  • sonciated vials and placed in oven at 3pm
    • programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs

Data/Spectra

  • Insert content here...

Notes

  • Insert content here...


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