User:Abigail E. Miller/Notebook/MOF Project/2013/01/25

Current revision

Metal Organic Frameworks

Added zinc nitrate hexahydrate, DPNI and TCPP to four vials.
- insert chart with weights here

added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4
- made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4
- added 250 μL of pure ethanol to vials 1-3

made a 10 mL solution of 1 M nitric acid in ethanol
- 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid
- --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol

sonciated vials and placed in oven at 3pm
- programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs

@@ Line 7: / Line 7: @@
 <!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
 ==Objective==
-* Insert content here...
+*Synthesis of PPF18 and PPF20
+* exchange PPf18 with adenine and guanine
+* make a stock solution of 1M HNO3 in ethanol
 ==Bench Work==
-* Insert content here...
+====exchanging PPF-18 with guanine and adenine====
+*
+====synthesizing PPF-18 and PPF-20====
+* Added zinc nitrate hexahydrate, DPNI and TCPP to four vials.
+** insert chart with weights here
+*added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4
+** made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4
+** added 250 μL of pure ethanol to vials 1-3
+*made a 10 mL solution of 1 M nitric acid in ethanol
+** 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid
+** --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol
+* added 100 μL of 1M HNO3 in EtOH to vials 1&2 and 80 μL to vials 3&4
+* sonciated vials and placed in oven at 3pm
+** programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs
 ==Data/Spectra==