Todd Lab - Revision history

Haseong Kim at 15:08, 24 October 2012

Haseong Kim — Wed, 24 Oct 2012 15:08:30 GMT

Matthew Todd — Thu, 09 Sep 2010 05:50:39 GMT

Matthew Todd — Thu, 09 Sep 2010 05:49:13 GMT

Removing all content from page

←Older revision		Revision as of 05:49, 9 September 2010
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-	~~==General Lab Protocols==~~

-	~~[[Standard metal salts to try for cyclam complex crystallisation]]~~
-
-	~~[[Chromatography]]~~
-
-
-	~~==Links==~~
-	~~[http://groups.chem.usyd.edu.au/todd/index.html Group Home Page]~~
-
-	~~[[User:Matthew Todd\|OWW Page for Mat Todd]]~~

Matthew Todd — Sun, 21 Jun 2009 03:40:29 GMT

←Older revision		Revision as of 03:40, 21 June 2009
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	==General Lab Protocols==		==General Lab Protocols==
-
-	~~Protocols are split up into the following areas:~~

	[[Standard metal salts to try for cyclam complex crystallisation]]		[[Standard metal salts to try for cyclam complex crystallisation]]

Matthew Todd — Sun, 21 Jun 2009 03:40:06 GMT

←Older revision		Revision as of 03:40, 21 June 2009
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-	==~~Other~~ Links==	+	==Links==
	[http://groups.chem.usyd.edu.au/todd/index.html Group Home Page]		[http://groups.chem.usyd.edu.au/todd/index.html Group Home Page]
		+
	[[User:Matthew Todd\|OWW Page for Mat Todd]]		[[User:Matthew Todd\|OWW Page for Mat Todd]]

Matthew Todd — Sun, 21 Jun 2009 03:39:48 GMT

←Older revision		Revision as of 03:39, 21 June 2009
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	[[Chromatography]]		[[Chromatography]]
		+
		+
		+	==Other Links==
		+	[http://groups.chem.usyd.edu.au/todd/index.html Group Home Page]
		+	[[User:Matthew Todd\|OWW Page for Mat Todd]]

Matthew Todd — Sun, 21 Jun 2009 03:37:05 GMT

←Older revision		Revision as of 03:37, 21 June 2009
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	==General Lab Protocols==		==General Lab Protocols==

-	~~Will need to~~ split ~~this page~~ up ~~with daughter pages~~	+	Protocols are split up into the following areas:

	[[Standard metal salts to try for cyclam complex crystallisation]]		[[Standard metal salts to try for cyclam complex crystallisation]]

	[[Chromatography]]		[[Chromatography]]

Matthew Todd — Sun, 21 Jun 2009 03:36:35 GMT

General Lab Protocols

←Older revision		Revision as of 03:36, 21 June 2009
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	[[Standard metal salts to try for cyclam complex crystallisation]]		[[Standard metal salts to try for cyclam complex crystallisation]]
		+
	[[Chromatography]]		[[Chromatography]]

Matthew Todd — Sun, 21 Jun 2009 03:36:22 GMT

←Older revision		Revision as of 03:36, 21 June 2009
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	[[Standard metal salts to try for cyclam complex crystallisation]]		[[Standard metal salts to try for cyclam complex crystallisation]]
-	~~Typical add-ins are PF6-, BF4-, Ph4B-, Cl4Zn2-. Usually use MeOH or MeCN as solvents for these.~~	+	[[Chromatography]]
-		+
-	~~Typical mixed-solvent diffusion tank methods are to dissolve the sample in MeCN, acetone, DMF or MeOH and allow ether to diffuse in.~~	+
-		+
-	~~Typical metals (generally) for cyclam recrysts are Cd, Ag (dark), Hg or Pb (usually sit on azamacrocycle, rather than in it). Fe(II)(BF4-)2 in MeCN is good.~~	+

Matthew Todd — Sun, 21 Jun 2009 03:33:08 GMT

←Older revision		Revision as of 03:33, 21 June 2009
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-
	==General Lab Protocols==		==General Lab Protocols==

	Will need to split this page up with daughter pages		Will need to split this page up with daughter pages

-	~~===~~Standard metal salts to try for cyclam complex crystallisation~~===~~	+	[[Standard metal salts to try for cyclam complex crystallisation]]
	Typical add-ins are PF6-, BF4-, Ph4B-, Cl4Zn2-. Usually use MeOH or MeCN as solvents for these.		Typical add-ins are PF6-, BF4-, Ph4B-, Cl4Zn2-. Usually use MeOH or MeCN as solvents for these.