Todd Lab

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(First addition of cyclam crystallisation methods)
Current revision (11:08, 24 October 2012) (view source)
 
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'''Todd Lab'''
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==General Lab Protocols==
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Will need to split this page up with daughter pages
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===Standard metal salts to try for cyclam complex crystallisation===
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Typical add-ins are PF6-, BF4-, Ph4B-, Cl4Zn2-. Usually use MeOH or MeCN as solvents for these.
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Typical mixed-solvent diffusion tank methods are to dissolve the sample in MeCN, acetone, DMF or MeOH and allow ether to diffuse in.
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Typical metals (generally) for cyclam recrysts are Cd, Ag (dark), Hg or Pb (usually sit on azamacrocycle, rather than in it). Fe(II)(BF4-)2 in MeCN is good.
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Current revision

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